Macromolecular Separation Science

Updated: 1 day ago
Location: Gaithersburg, MARYLAND
Deadline: The position may have been removed or expired!

NIST only participates in the February and August reviews.


Research focuses on the development and application of advanced multi-detector separation science techniques. Topics include characterizing the phase space inhabited by complex macromolecules and blends, nano/microplastics, nanoparticles, and carbohydrates. This will be done primarily using size-based separation methods such as SEC, AF4, and HF5, in conjunction with interaction polymer chromatography techniques such as i-GPEC and LCCC, coupled to a variety of on-line detection methods, including MALS, QELS, VISC, fluorescence, ICP-MS, Raman, etc. Exploring the fundamentals of the separation and detection methods is also part of this opportunity.

References

Striegel AM: On-line coupling of hollow-fiber flow field-flow fractionation and depolarized multi-angle static light scattering (HF5/D-MALS). Proof of principle. Journal of Chromatography A 1739:465115 2024

Striegel AM: Absolute molar mass determination in mixed solvents. 2. SEC/MALS/DRI in a mix of two "nearly-isovirial" solvents. Analytica Chimica Acta 1231:340369, 2022

Striegel AM: Method development in interaction polymer chromatography. Trends in Analytical Chemistry 130:115990, 2020

Pitkänen L, Montoro Bustos AR, Murphy KE, Winchester MR, Striegel AM: Quantitative characterization of gold nanoparticles by size-exclusion and hydrodynamic chromatography, coupled to inductively coupled plasma mass spectrometry and quasi-elastic light scattering. Journal of Chromatography A 1511: 59-67, 2017

Pitkänen L, Striegel AM: Polysaccharide characterization by hollow-fiber flow field-flow fractionation with on-line multi-angle static light scattering and differential viscometry. Journal of Chromatography A 1380:146-155, 2015


Separation science; Multiple detection; Multi-dimensional; Macromolecules; Polymers, Carbohydrates; Nanoparticles; Polysaccharides; Liquid chromatography;

Citizenship:  Open to U.S. citizens



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